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NMR Studies and Crystal Structure Determinations of CF3 Group-containing Bicyclic phenolates

Mamat, C.; Reinke, H.; Langer, P.

Abstract

Three new CF3-substituted bicyclic Salicylate derivatives were synthesized by the TiCl4-mediated cyclization Of trifluoromethyl-containing ketones with 1,3-bis(silyl enol ethers) and characterized by NMR and IR, spectroscopy, Mass spectrometry and elemental analysis. The crystal structures of the bicyclic derivatives have been determined by single crystal X-ray analysis. All structures exhibit hydrogen bonding.

  • Zeitschrift für Naturforschung Section B - A Journal of Chemical Sciences 64(2009)4, 423-426
    ISSN: 0932-0776

Permalink: https://www.hzdr.de/publications/Publ-13252


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